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3.2. XRD analyses XRD measurements were performed at CEREGE on powdered samples with a q-q Panalytical X Pert Pro MPD diffractometer running at 40 kV and 40 mAusing Co Ka radiation (l ¼ 1.79A) with a linear X Celerator detector and a secondary ﬂat monochromator. The 2q range was 23e75 with a step size of 0.033 and a counting
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X-ray Diffraction (XRD) X-ray diffractometer A powerful way to identify crystalline materials. The physical basis is Bragg s Law (a Nobel prize for simple trigonometry). The angles required for diffraction and the intensity of the diffracted wavelengths can be used to identify the material.
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